Working group “Rheometry”

Measuring the rheological properties of fresh building materials such as cement paste, mortar or concrete is a very challenging task. In contrast to many other substances, building materials consist of a very wide particle size distribution, with particles ranging from the sub-micron range to the double-digit millimeter range. In (standard) rheological measurements, this results in the formation of slippage layers and segregation, which spoil the rheological measurement. Further, concrete, mortar and paste are chemically highly reactive systems, which leads to sometime pronounced problems in carrying out rheological measurements on such systems.

Goals

Working Group Rheometry in SPP 2005 addresses these questions by investigating and comparing the different measurement techniques available for cementitious systems. In detail, WG Rheometry has the following goals:

  • Provide a comparison and evaluation for the rheological measurement techniques available and used by the SPP members;
  • Study of comparability of different rheological measurement geometries;
  • Study in-situ measurement techniques, combining rheological and granulometrical/chemical measurements;
  • Provide scale bridging quantified evaluations of rheology.
Goals of working group rheometry
© DFG-SPP-2005

Members & Institutions

Chair

  • Michael Haist
    Leibniz University Hannover, Germany

Current Members

  • Claudia Crasselt
    Bundesanstalt für Materialforschung und –prüfung (BAM), Germany
  • Mahmoud Eslami Pirharati
    Technische Universität Braunschweig, Germany
  • Roxana Figuli
    Karlsruhe Institute of Technology (KIT), Germany
  • Irina Ivanova
    Technische Universität Dresden, Germany
  • Christopher Klein
    Karlsruhe Institute of Technology (KIT), Germany
  • Thomas Kränkel
    Technical University Munich, Germany
  • Sarah Leinitz
    Bundesanstalt für Materialforschung und –prüfung (BAM), Germany
  • Julian Link
    Leibniz University Hannover, Germany
  • Dirk Lowke
    Technische Universität Braunschweig, Germany
  • Inka Mai
    Technische Universität Braunschweig, Germany
  • Viktor Mechtcherine
    Technische Universität Dresden, Germany
  • Tamara Meyer
    Karlsruhe Institute of Technology (KIT), Germany
  • Alexander Mezhov
    Bundesanstalt für Materialforschung und –prüfung (BAM), Germany
  • Daniil Mikhalev
    Technische Universität Dresden, Germany
  • David Nicia
    Technische Universität Braunschweig, Germany
  • Ursula Pott
    Technische Universität Berlin, Germany
  • Silvia Reißig
    Technische Universität Dresden, Germany
  • Wolfram Schmidt
    Bundesanstalt für Materialforschung und –prüfung (BAM), Germany
  • Dietmar Stephan
    Technische Universität Berlin, Germany
  • Bastian Strybny
    Leibniz University Hannover, Germany
  • Mareike Thiedeitz
    Technical University Munich, Germany
  • Christian Vogel
    Leibniz University Hannover, Germany
  • Manfred Wilhelm
    Karlsruhe Institute of Technology (KIT), Germany

Former Members

  • Shirin Fataei
    Technische Universität Dresden, Germany
Insitutions of working group rheometry

Group meetings

Date

Location

June 2018

Karlsruhe

December 2018

Frankfurt

February 2019

Berlin

May 2019

Hannover

October 2019

Online

December 2019

Online

May 2021

Online

July 2021

Online

November 2021

Online

May 2022

Online

Results and Current Work

A major achievement of the working group resulted in a paper dealing with an interlaboratory study of the rheological properties of cement paste and ultrasound gel as reference substance. The main goal was to quantify the comparability and reproducibility of measurements of the Bingham parameters yield stress and plastic viscosity when measured on one specific paste composition and one particular ultrasound gel in different laboratories using various rheometers and measurement geometries. The procedures for both in preparing the cement paste and performing the rheological measurements on cement paste and ultrasound gel were carefully defined for all of the study’s participants. Different conversion schemes for comparing the results obtained with the different measurement setups are presented here and critically discussed. The procedure proposed in this paper ensured a reasonable comparability of the results with a coefficient of variation for the yield stress of 27% and for the plastic viscosity of 24%, despite the individual measurement series’ having been performed in different labs with different rheometers and measurement geometries.

Development of generalised data conversion
© DFG-SPP-2005

Currently, a new test series on in-situ measurement techniques is being evaluated. Here, a focus is set on analytical studies of granulometry and chemical composition during rheological measurements. For this purpose, results of the Focused Beam Reflectance Measurement (FBRM), Electrosonic Amplitude (ESA), Rheomicroscopy, Rheo-Raman, Rheo-NMR and other measurement methods of cement suspensions are combined and correlated. The objective is to gain a deeper understanding of changes of the particulate state within a cement suspension during applied shear load.

Publications

M. Haist, J. Link, D. Nicia, S. Leinitz, C. Baumert, T. von Bronk, D. Cotardo, M. Eslami Pirharati, S. Fataei, C. Gehlen, I. Hauschildt, I. Ivanova, S. Jesinghausen, C. Klein, H.-W. Krauss, L. Lohaus, D. Lowke, O. Mazanec, S. Pawelczyk, U. Pott, N.W. Radebe, J. J. Riedmiller, H.-J. Schmid, W. Schmidt, E. Secrieru, D. Stephan, M. Thiedeitz, M. Wilhelm, V. Mechtcherine

Materials and Structures 53 (2020)